Expedient Synthesis of Phenanthro-Imidazo-Pyridine Fused Heteropolynuclear Framework via CDC coupling: A New Class of Luminophores

Banerji, Biswadip and Chatterjee, Satadru and Chandrasekhar, K and Bera, Suvankar and Mazumder, Leena and Prodhan, Chandraday and Chaudhuri, Keya (2017) Expedient Synthesis of Phenanthro-Imidazo-Pyridine Fused Heteropolynuclear Framework via CDC coupling: A New Class of Luminophores. Organic & Biomolecular Chemistry, 15 (19). pp. 4130-4134.

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    Abstract

    All the reagents and solvents used in this study, were purchased from Sigma Aldrich, Thermo Fischer Scientific and TCI chemicals respectively. Open capillary was used to measure all the melting points. IR spectrum of the solid sample was recorded in the range 500 to 3500 cm-1 in an FT-IR spectrometer in KBr cell. Bruker 600 MHz spectrometer was used to record all 1H and 13C NMR spectra. EI mass spectral analysis was done using JEOL The Mstation JMS-700 instrument. All the UV & Fluorescence data were collected using Jasco & Cary Eclipse spectrophotometer respectively. Bruker Kappa Apex II X-raycrystallography machine was used to solve the crystal structure. Singlet (s), doublet (d), triplet (t) & multiplet (m) were designated as 1H NMR multiplicity patterns. Silica gel (60-120 mesh) and (100-200 mesh) were used for column chromatographic separations.

    Item Type: Article
    URI: http://www.eprints.iicb.res.in/id/eprint/2666
    Subjects: Chemistry
    Molecular & Human Genetics
    Divisions: Indian Institute of Chemical Biology
    Depositing User: Ms Sutapa Ganguly
    Date Deposited: 06 Jun 2017 16:56
    Last Modified: 06 Jun 2017 16:56
    Official URL: http://dx.doi.org/10.1039/C7OB00564D
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